Cov txheej txheem ntxaws ntxaws rau kev rho tawm myrrh tseem ceeb roj

Qhov no yog ib qho kev txhim kho ib txwm muaj.

Cov kauj ruam tshwj xeeb

• Crushing thiab nthuav dav: Siv ib lub micro crusher nruab nrog a1.8mm aperture sieveTxhawm rau txhawm rau hauv MyRrh, ua raws li los ntawm kev kho kom nthuav dav hauv lub tshuab nthuav dav ntawm65 Degree(rau 30-80 feeb). Cov kauj ruam no pab cuam tshuam cov qauv ntawm tes thiab txhim kho cov roj ntxiv tseem ceeb.
• Kev Txiav Txim Siab:'S crushed thiab nthuav myrrh hmoov yog concentrated siv cov teb chaws araporator kom tau txais cov pos hniav, uas yog tom qab ntawd thiaj li muaj kev sib cavdiethil etherCov. Lub hom phiaj yog kom tshem tawm qee cov resins thiab impurities, txo kev cuam tshuam rau cov kauj ruam tom ntej.
• Distillation Extraction: Qhov kev sib tw myrrh raug xa mus rau qhov chaw ua haujlwm distillation,60% concentration ethanolyog ntxiv (myrrh rau Ethanol pawg piv ntawm 1: 7), thiabPeb ncig ntawm distillationyog ua:

Thawj distillation: 40 feeb

Thib ob distillation: 30 feeb

Peb distillation thib peb: 22 feeb. Cov kev rho tawm los ntawm tag nrho peb puag ncig yog ua ke kom tau txais cov crudh morrh extract.

• Kev xav thiab kho kom zoo: Cov ntaub ntawv txiav txim siab yog lim kom tshem cov seem, tom qab ntawd qhuav thiab feeb kom tau txais cov tshuaj ntsuab zoo kawg nkaus.

Qhov no yog qhov niaj hnub, kev siv thev naus laus zis ntau heev.

Cov kauj ruam tshwj xeeb

• Kev daj: Lub ntsej muag nyoos myrrh cov khoom yog crushed rau hauv cov hmoov.
• Supercritical Extraction: 10-20 ntu (los ntawm qhov hnyav) ntawm myrrh hmoov yog muab tso rau hauv aSupercritical suav rho tawm ApparatusCov. Extraction yog nqa tawm rau3-5 teevnyob rau hauv cov xwm txheej ntawmSiab 12-14 MPA, Kub 50-54 Qib, thiabTus Nqi Flow Flow 3-5 L / Kg H.
• Tsawg - kev sib hais daws thiab pom kev: Cov tau txais cov extract yog sab laug sawv ntawm4℃rau 23-25 ​​teev, tom qab ntawd lim thiab feeb meej hauv qab kev txo qis kom tau txais cov tshuaj txhuam tawm.
• Huv: Tus muab tshuaj txhuam tau sib cais sivSilica gel kem chromatography, eluted sib npaug nrogdichhloromethane - methanolKev daws teeb meem ntawm kev sib txawv sib piv. Tus22: 1 Kev Nyab Xeeb Kev Nyab Xeebyog sau thiab muaj lub siab kom tau txais lub huv myrrh molatile roj roj fab.

Qhov zoo ntawm hom noyuavKev Tawm Tsam Ntau, luv luv lub sijhawm ua tiav, thiab tau txais cov roj roj scatileQhia qhov tseem ceeb anti - qog nqaij, ua rau nws tsim nyog rau kev npaj khoom lag luam.

Qhov no yog ib qho qauv qub classic rau kev rho tawm cov roj tseem ceeb los ntawm ntau cov nroj tsuag, nrog nws cov txheej txheem tsis zoo kuj tau ua kom zoo los ntawm kev tshawb fawb.

Siv txheej txheem tsis txheeb

• Cov khoom -} kua piv: Qhov sib piv ntawm myrrh rau dej feem ntau1:5(Qhov hnyav / ntim piv).
• Soaking sijhawm: 0.5 teev(Kev tshawb fawb qhia tau tias tsis muaj tog so los yog luv ntxuav lub sijhawm muaj txiaj ntsig zoo rau kev rho tawm ntawm cov roj volatile).
• Extract lub sijhawm: 8 teev(Kev tshawb fawb pom tias 8 teev ntawm extraction yields zoo tshaj 6 teev).

Cov txheej txheem luv luv

Cov txheej txheem hauv Myrrh yog tov nrog dej, thiab chav kawm tau qhia rau cua sov, ua rau cov roj hloov hluav taws xob kom yaj nrog lub chav. Lub vapor yog tom qab ntawd condensed rov qab rau hauv cov kua ntawm lub condenser, thiab cov roj tseem ceeb tau sib cais los ntawm cov dej raws li kev ntom ntom ntom ntom.

Qhov zoo ntawm hom noyog cov khoom siv tau yooj yim thiab cov cai,tsis muaj cov txheej txheem organic, thiab haum rau ib txwm thiab cov khoom lag luam uas muaj. Qhov tsis zoo suav nrogLub sijhawm siv sijhawm ntevthiablos ntawm qis qis ntxiv cov txiaj ntsig.

Cov lus hauv qab no taw tes ua rau cov yam ntxwv ntawm cov hau kev tseem ceeb rau kev sib piv yooj yim:

Cov lus qhia xaiv

• Yog tias koj yog cov roj tsim hluav taws xob tseem ceeb lossis xav sim hauv tsev: TusChav Didillation Chavyog yuav ua tau zoo tshaj plaws thiab kev nyab xeeb tshaj plaws (zam kev siv cov organic cov kuab tshuaj zoo li diethyl ether ether). Nco ntsoov ua ntej kev nyab xeeb, siv cov iav khob iav tsim nyog thiab cua sov tswj.
• Yog tias koj khiav ib lub studio me me lossis rooj cob qhia me me: Koj yuav txiav txim siab simDistillation extraction txoj kev, tab sisKev Nyab Xeeb yog Paramount, tshwj xeeb tshaj yog thaum siv thiab rov ua cov tshuaj organic zoo li diethyl ether thiab ethanol, uas yog cov nplaim taws thiab tawg. Kev ua haujlwm yuav tsum tau ua nyob rau hauv ib tug zoo - pa nqus ib puag ncig adhery rau kev nyab xeeb kev nyab xeeb kev nyab xeeb.
• Rau Industrial - nplai ntau lawm lossis tshawb fawb: Txawm tias tusSupercritical suav cov txheej txheem rho tawmYuav tsum muaj qhov tseem ceeb hloov tshiab kev nqis peev, nws txoj kev ua haujlwm siab thiab siab - cov khoom lag luam zoo yuav muaj cov txiaj ntsig zoo dua.
• Tsis hais tus qauv, tusZoo ntawm lub RAW MYRRH(hauv paus chiv keeb, keeb kwm, kev cia khoom) yuav cuam tshuam cov roj kawg thiab zoo.

• Kev Nyab Xeeb Ua Ntej: Cov txheej txheem rho tawm yuav muaj cov kev ntsuas kub, siab, thiab cov nplaim hluav taws xob / cov tshuaj lom neeg zoo li diethyl ether, ethanol).Ib txwm ua haujlwm nyob rau hauv ib tug zoo - pa taws chaw, thiab hnav cov khoom tiv thaiv uas tsim nyog (zoo li tsom iav, kev nyab xeeb tsom iav)Cov. Yog tias koj tsis muaj kev paub dhau los, nws tau qhia kom muaj tseeb kom ua raws li kev taw qhia ntawm tus kws tshaj lij.
• Tau qhov twg los cov ntaub ntawv raw: Xyuas kom cov sivhigh - Zoo, tsis ua kom tsis tau txais kuv lub resinraws li cov khoom siv raw. Cov qhab nia sib txawv thiab cov chaw ntawm cov khoom siv raw yuav cuam tshuam rau cov roj tawm thiab cov tshuaj muaj kuab lom.
• Cov Cai thiab Cov Cai: Yog tias koj npaj yuav tsim lossis muag myrrr
• Tseem Ceeb Roj Cia: Lub npaj myrrh tseem ceeb roj yuav tsum muab cia rau hauvCov iav tsaus nti iav, ntim thiab tiv thaiv los ntawm lub teeb, hauv qhov chaw txiasTxhawm rau txuas nws lub txee lub neej thiab tswj kom zoo.